Forensic and Clinical Applications of Solid Phase Extraction
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ISBN-13:
9781617371141
Veröffentl:
2010
Einband:
Paperback
Erscheinungsdatum:
19.11.2010
Seiten:
384
Autor:
Michael J. Telepchak
Gewicht:
721 g
Format:
254x178x21 mm
Serie:
Forensic Science and Medicine
Sprache:
Englisch
Beschreibung:
This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.
Includes supplementary material: sn.pub/extras
Introduction to Solid Phase ExtractionSilica-Based Solid Phase ExtractionThe Chemistry of Bonded SilicasBonded Phase Sorbent SynthesisStrategies for the Use of Solid Phase ExtractionOptimizing Solid Phase Extraction MethodsSeparation of Analytes from Their MatricesSolid Phase Extraction TroubleshootingDrug Methods for the Toxicology LabSelected Solid Phase Extraction Applications in Drug AnalysisGeneral Methods for Drug IsolationChemical DerivatizationAppendix A: GlossaryAppendix B: ReagentsAppendix C: Preparation of Solutions and BuffersAppendix D: Milliequivalent and Millimode CalculationsAppendix E: Selected Solvent Polarity and Property ScaleAppendix F: Buffers for Solid Phase ExtractionAppendix G: pKa Reference for Solid Phase ExtractionAppendix H: RapidTrace® Operation GuideAppendix I: Further Reading
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