Beschreibung:
Handbook of Synthetic Organic Chemistry, Second Edition updates and expands the author's popular 2007 work, Synthetic Organic Chemist's Companion. This new handbook provides valuable, practical guidance; incorporates corrections, and includes coverage on important topics, such as lyophylization, crystallization, precipitation, HPLC detectors, gases, and microwave reactions.
1. Safety 2. Searching the Literature 3. Reagents 4. Gases 5. Reactions on a Small Scale-1-25mmol 6. Temperature Control 7. Solvents 8. The Research Notebook 9. Conducting the Reaction Itself 10. Following the Reaction 11. Working Up Reactions 12. Evaporation 13. Vacuum Systems 14. Purification of Products 15. Methods for Structure Elucidation 16. Cleaning Up After the Reaction 17. Specific Example 18. Strategies for Reaction Optimization